KMID : 0369819740040010101
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Jorunal of Korean Pharmaceutical Sciences 1974 Volume.4 No. 1 p.101 ~ p.106
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Identification and Spectrophotometric Method for Determination of the ¥â- Fluorine Compounds in Fluorides of Ethanol and its Ester
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½É¿µ±â/Sim YK
ÀÌÇÑÇ¥/±¸±â¼/±èÀç¹é/Lee HP/Ku KS/Kim JB
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Abstract
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S-Benzylthiuronium chloride reacts with ethylene glycol, derived from hydrolysis of the fluorides, to produce a crystalline substances. Using this, the fluorides can be indentified by measuring melting point. And when the zirconium-alizarin solution reacts with ethylenefluoro hydrin or ${\beta}-fluoroethyl$ ¼ö½Ä À̹ÌÁö acetate, the red-violet color disappears to produce a yellow dye, which exhibits absorption maximum at about $530\;m{\mu}$ ¼ö½Ä À̹ÌÁö using the 250-microgram standard. Using these properties, the fluorine compounds can be determined conveniently by this method.
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KEYWORD
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